HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxybenzenesulfonyl chloride → 8-(4-Methoxybenzenesulphonamido)octanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| Reactant | 8-Aminooctanoic acid | HCID 66085 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | 8-(4-Methoxybenzenesulphonamido)octanoic Acid | HCID 20066968 | — |
Reaction Steps
A solution of 8-aminooctanoic acid in 10% sodium hydroxide solution was treated with 4-methoxybenzenesulphonylchloride in the manner of Example 2 to give the title compound which, on recrystallisation from aqueous 2-propanol, had a melting point of 102°-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997847 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-f5f8b95cdb084ebe9d17e567654ad659 |
| Source note | uspto-grants-1991_03 |