HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonyl chloride → 11-(4-Chlorobenzenesulphonamido)undecanoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| Reactant | 11-Aminoundecanoic acid | HCID 17083 | — |
| Product | 11-(4-Chlorobenzenesulphonamido)undecanoic Acid | HCID 13192138 | — |
Reaction Steps
11-Aminoundecanoic acid (4.02 g, 0.02 mol) was treated with 4-chlorobenzenesulphonyl chloride (4.22 g, 0.02 mol) as described in Example 4 to give the title compound which was recrystallised from 2-propanol/ether (1.8 g, m.p. 128°-9° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997847 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-2f0ef4b2716e48929b1b45aec994ea09 |
| Source note | uspto-grants-1991_03 |