HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20066966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20066941 | HCID 20066941 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20066966 | HCID 20066966 | — |
Reaction Steps
9-(3-Chlorobenzenesulphonamido)nonanenitrile (4.4 g, 0.013 mol) was treated with NaOH (5 g, 0.115 mol) in 30 ml water and 50 ml ethanol by the method described in Example 6(ii). Chromatography in CHCl3 :MeOH 10:1 on silica and recrystallisation from 2-propanol/pet. ether 60°-80° gave the title compound (0.94 g, m.p. 112°-3° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997847 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-fc46a4b89fa74ac285c7e124d1429a96 |
| Source note | uspto-grants-1991_03 |