HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 20066945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 20066976 | HCID 20066976 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20066945 | HCID 20066945 | — |
Reaction Steps
9-(4-Bromobenzenesulphonamido)nonanenitrile (0.6 g, 0.0016 mol) was treated with sodium hydroxide (2 g, 0.05 mol) in 10 ml water plus 20 ml ethanol by the method described in Example 6(ii) to give the title compound (0.35 g, m.p. 124°-5° C.) after recrystallisation from chloroformpetroleum ether 40°-60°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997847 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-53a1bf167b104335b03ad347e668ac8d |
| Source note | uspto-grants-1991_03 |