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HRID358647

反应详情

EQUATION

反应方程式

HRID 358647 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：NS(=O)(=O)c1ccc(Cl)cc1
HCID66824

4-Chlorobenzenesulphonamide

C6H6ClNO2S

结构：CCOC(=O)C(C)(C)CCCCCCCBr
HCID11369854

Nonanoic acid, 9-bromo-2,2-dimethyl-, ethyl ester

C13H25BrO2

PRODUCTS

生成物

1
结构：CCOC(=O)C(C)(C)CCCCCCCNS(=O)(=O)c1ccc(Cl)cc1
HCID20066938

未命名化合物

收率 53%

PROCEDURE

实验过程

Ethyl 2,2-dimethyl-9-bromononanoate (2.0 g, 0.007 mol) was treated with 4-chlorobenzenesulphonamide (3.44 g, 0.018 mol) and potassium carbonate (6.2 g, 0.045 mol) by the method described in Example 5(ii) to give the title compound (1.5 g) as an oil.