huagongshe.com
HRID358649

反应详情

EQUATION

反应方程式

HRID 358649 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：NS(=O)(=O)c1ccc(Cl)cc1
HCID66824

4-Chlorobenzenesulphonamide

C6H6ClNO2S

结构：CCOC(=O)C(C)(C)CCCCCBr
HCID11265571

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)C(C)(C)CCCCCNS(=O)(=O)c1ccc(Cl)cc1
HCID20066981

未命名化合物

收率 13.3%

PROCEDURE

实验过程

Ethyl-2,2-dimethyl-7-bromoheptanoate (7.0 g, 0.026 mol) was treated with 4-chlorobenzenesulphonamide (9.9 g, 0.052 mol) and potassium carbonate (21.5 g, 0.016 mol) by the method described in Example 5(ii) to give the title compound (1.3 g) as an oil.