HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Ethyl-7-(4-chlorophenylsulphonamido)-2,2-dimethylheptanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Chlorobenzenesulfonamide | HCID 66824 | — |
| Reactant | Ethyl 7-bromo-2,2-dimethylheptanoate | HCID 11265571 | — |
| Product | Ethyl-7-(4-chlorophenylsulphonamido)-2,2-dimethylheptanoate | HCID 20066981 | 13.3% |
Reaction Steps
Ethyl-2,2-dimethyl-7-bromoheptanoate (7.0 g, 0.026 mol) was treated with 4-chlorobenzenesulphonamide (9.9 g, 0.052 mol) and potassium carbonate (21.5 g, 0.016 mol) by the method described in Example 5(ii) to give the title compound (1.3 g) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997847 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-5da6c82ea9584078a688cc061d641b84 |
| Source note | uspto-grants-1991_03 |