Iodoethane → HCID 67903479, compound

Participants

Reaction Steps

A mixture of the compound prepared in example 9 (0.3 g, 0.61 mmol) and ethyl iodide (2 mL) dissolved in acetonitrile (1 mL) was refluxed under argon atmosphere for 12 h. The mixture was permitted to cool, the solvent was evaporated in vacuo and the residue was recrystallized with dichloromethane and diethyl ether to yield 0.36 g of the title compound of this example as a yellowish solid (90% yield).

Provenance & Evidence