HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-(bromomethyl)-3-methoxybenzoate → HCID 19744336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-(bromomethyl)-3-methoxybenzoate | HCID 2759828 | — |
| Reactant | 5-bromo-6-nitro-1H-indole | HCID 19744331 | — |
| Product | HCID 19744336 | HCID 19744336 | 65% |
Reaction Steps
5-Bromo-6-nitroindole was reacted with methyl 4-bromomethyl-3-methoxybenzoate using the procedure described in part (a) of Example 1 to give methyl 4-(5-bromo-6-nitroindol-1-ylmethyl)-3-methoxybenzoate (HH) in 65% yield and as a bright yellow solid; partial NMR: 3.89 (s,3H,OCH3), 3.94 (s,3H,OCH3), 5.35 (s,2H,NCH2), 6.53 (dd,1H,H3 -indole), 7.38 (d,1H,H2 -indole), 7.89 (s,1H,H4 -indole), 8.03 (br s,1H,H7 -indole).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04997844 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-8db670433ffb46d78ad17f9eed893870 |
| Source note | uspto-grants-1991_03 |