HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 14580088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | [5-(Acetyloxy)-4,6,7-trimethyl-2,3-dihydro-1-benzofuran-2-yl]acetic acid | HCID 65961 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 14580088 | HCID 14580088 | — |
Reaction Steps
To a suspension of (RS)-2-(2,3-dihydro-5-acetyloxy-4,6,7-trimethylbenzofuranyl) acetic acid (see example 2) (4.4 g) in benzene (36 ml) is added dropwise oxalyl chloride (7 ml) over 30'.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04999350 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-52188ab80e9b4b34b4c1a803b10ee522 |
| Source note | uspto-grants-1991_03 |