Potassium Carbonate → HCID 67796181, compound

HRID 358965Notes

Reaction equation

HRID 358965 reaction equation
[N:1]1([CH2:7][CH:8]2[C:20]3[C:19]4[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=4[NH:13][C:12]=3[CH2:11][CH2:10][NH:9]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C(=O)([O-])[O-].[K+].[K+].[Cl:27][C:28]1[CH:29]=[C:30]([CH2:35][C:36](Cl)=[O:37])[CH:31]=[CH:32][C:33]=1[Cl:34]>C(Cl)(Cl)Cl>[N:1]1([CH2:7][C:8]2([C:36](=[O:37])[CH2:35][C:30]3[CH:31]=[CH:32][C:33]([Cl:34])=[C:28]([Cl:27])[CH:29]=3)[C:20]3[C:19]4[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=4[NH:13][C:12]=3[CH2:11][CH2:10][NH:9]2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 27581492-(3,4-Dichlorophenyl)acetyl chlorideHCID 20065694HCID 20065694, compound

Product 1

HCID 67796181HCID 67796181, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Prepared as Ex. No. 12, from 1.1 g (4.08 mmoles) of crude 1-(piperidin-1-yl)methyl-1,2,3,4-tetrahydro-5H-pyrido[4,3-b]indole, 1.12 g (8.10 mmoles) of anhydrous potassium carbonate and 1.1 g (4.92 mmoles) of 3,4-dichlorophenylacetylchloride in 40 ml of dry chloroform.

Workup

  1. customPrepared as Ex

Sources & evidence

ORD record
ord-efc5f2bb4ed44b9ca9b35831344c72ad
Source dataset
uspto-grants-1991_03
Patent number
US04999359

Reaction notes

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