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HRID358969

反应详情

EQUATION

反应方程式

HRID 358969 的结构方程式

REACTANTS

反应物

2
结构：O=C(C1NCCc2[nH]cnc21)N1CCCC1
HCID20065693

未命名化合物

结构：[Al+3].[H-].[H-].[H-].[H-].[Li+]
HCID21226445

未命名化合物

PRODUCTS

生成物

1
结构：c1nc2c([nH]1)CCNC2CN1CCCC1
HCID20065697

4-(Pyrrolidin-1-yl)methyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridine

C11H18N4

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

3.63 g (16.48 mmoles) of 4-(pyrrolidin-1-yl)carbonyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridine were added portionwise, at room temperature, under nitrogen atmosphere, to a slurry of 1.00 g (26.32 mmoles) of lithium aluminium hydride in 180 ml of dry dioxane.