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HRID 358969作成日：2026年10月25日

4-(Pyrrolidin-1-yl)carbonyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridine → 4-(Pyrrolidin-1-yl)methyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridine

https://huagongshe.com/reaction/358969

反応式

関与物質

役割名称HCID仕込み量
反応物4-(Pyrrolidin-1-yl)carbonyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridineHCID 20065693—
反応物Aluminium lithium hydrideHCID 21226445—
溶媒1,4-DioxaneHCID 31275—
生成物4-(Pyrrolidin-1-yl)methyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridineHCID 20065697—

反応手順

3.63 g (16.48 mmoles) of 4-(pyrrolidin-1-yl)carbonyl-4,5,6,7-tetrahydroimidazo[4,5-c]pyridine were added portionwise, at room temperature, under nitrogen atmosphere, to a slurry of 1.00 g (26.32 mmoles) of lithium aluminium hydride in 180 ml of dry dioxane.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04999359
出典データセットuspto-grants-1991_03
ORD IDord-3f8afb5197e244b2905297b9140d96b2
出典メモuspto-grants-1991_03