HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 15170292, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | 10H-[1]Benzothieno[3,2-b]indole | HCID 354261 | — |
| Solvent | Methylenechloride Hexane | HCID 21226440 | — |
| Product | HCID 15170292 | HCID 15170292 | 91.9% |
Reaction Steps
Using the procedure outlined in Example 34A except that dimethyl sulfate was used as the alkylating agent, 10H-[1]benzothieno[3,2-b]indole (prepared by the method of K. E. Chippendale and B. Iddon, JCS Perkin Trans. I, 2023 (1972)) gave a 91.9% yield of 10-methyl-10H-[1]benzothieno[3,2-b]indole, mp 175°-176°, (CH2Cl2 /hexane), (C,H,N,S).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04999369 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-4be274b2a3404dd9870b94ec7e1adef5 |
| Source note | uspto-grants-1991_03 |