Toluene → HCID 20064754, compound

Participants

Reaction Steps

By the procedure of Example 15, 4.84 g (0.04 mol) of 2,6-dimethyl aniline was added to a stirred solution of 75 ml toluene containing 4.87 g (0.02 mol) of 2-chloro-4-trifluoromethyl-5-oxazolecarboxylate. The reaction mixture was stirred at reflux for 24 hours. The product was separated, distilled and then recrystallized from petroleum ether to yield 1.99 g of crystal product (m.p.=79°-81° C.) identified in Table I.

Provenance & Evidence