HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 1-(2-phenylethyl)-1,4,5,6-tetrahydro-3-pyridyl ketone → Propyl 1-propyl-1,4,5,6-tetrahydro-3-pyridyl ketone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 1-(2-phenylethyl)-1,4,5,6-tetrahydro-3-pyridyl ketone | HCID 18963355 | — |
| Reactant | 1-(2-Propenyl)-3-butyryl pyridinium bromide | HCID 18963365 | — |
| Product | Propyl 1-propyl-1,4,5,6-tetrahydro-3-pyridyl ketone | HCID 18963391 | — |
Reaction Steps
1-(2-Propenyl)-3-butyryl pyridinium bromide was hydrogenated according to the procedure described in Part (b) of Example 6 to give propyl 1-propyl-1,4,5,6-tetrahydro-3-pyridyl ketone. The product was distilled as a pale yellow oil (b.pt 150-153°C./0.3 mm Hg)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05000946 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-e3f19aebb1074bc7ac4c7ff0c47d1fae |
| Source note | uspto-grants-1991_03 |