4-Butylbenzoyl chloride → HCID 20064880, compound

HRID 359337Notes

Reaction equation

HRID 359337 reaction equation
[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[NH:9][CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1.[CH2:14]([C:18]1[CH:26]=[CH:25][C:21]([C:22](Cl)=[O:23])=[CH:20][CH:19]=1)[CH2:15][CH2:16][CH3:17].CC(N1CCCC(C(C)=O)=C1)C>>[CH3:1][C:2]1([CH3:13])[CH2:11][C:10]2[N:9]([C:22](=[O:23])[C:21]3[CH:25]=[CH:26][C:18]([CH2:14][CH2:15][CH2:16][CH3:17])=[CH:19][CH:20]=3)[CH2:8][CH2:7][CH2:6][C:5]=2[C:4](=[O:12])[CH2:3]1

Participants

4

Reactant 3

HCID 1200494-Butylbenzoyl chlorideHCID 118196217,7-Dimethyl-2,3,4,6,7,8-hexahydroquinolin-5(1H)-oneHCID 18963350HCID 18963350, compound

Product 1

HCID 20064880HCID 20064880, compound

Procedure

7,7-Dimethyl-1,2,3,4,7,8-hexahydro-quinoline -5(6H)-one was reacted with 4-butylbenzoyl chloride according to the procedure of Part (b) of Example 1 to give 7,7-dimethyl-1,2,3,4, 7,8-hexahydro-1-(4-butylbenzoyl)-quinoline5(6H)-one (22) as a yellow solid.

Sources & evidence

ORD record
ord-fd8e420273c74bffbf01473d2cc70f2e
Source dataset
uspto-grants-1991_03
Patent number
US05000946

Reaction notes

Loading…