HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isothiocyanate → HCID 15135525, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | 2-Amino-N-methylbenzamide | HCID 308072 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 15135525 | HCID 15135525 | 87.9% |
Reaction Steps
To a stirred mixture of 12 g of 2-amino-N-methylbenzamide and 200 ml of ether was added dropwise, a solution of 13.1 g of benzoyl isothiocyanate in 100 ml of ether over 30 minutes. The solid was collected, giving 22 g of the desired product as cream-colored crystals, mp 203°-205° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001157 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-612126bdaac440fc8e5787c1f62b3aec |
| Source note | uspto-grants-1991_03 |