HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilamide → HCID 797250, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | 2-Methylbenzoyl isothiocyanate | HCID 141396 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 797250 | HCID 797250 | 95.8% |
Reaction Steps
To a stirred mixture of 4.9 g of 2-aminobenzamide and 200 ml of ether was added dropwise, a solution of 6.67 g of 2-methylbenzoyl isothiocyanate in 100 ml of ether over 15 minutes After a few hours, the solid was collected, giving 10.8 g of the desired product as grey crystals, mp 181°-185° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001157 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-4b38721960304ccfa0f1595365e708ac |
| Source note | uspto-grants-1991_03 |