HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → N-[2-(2-methylpropoxy)phenyl]-3-(trifluoromethyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(Trifluoromethyl)benzoyl chloride | HCID 67561 | — |
| Reactant | (2-Isobutoxyphenyl)amine | HCID 13654662 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | N-[2-(2-methylpropoxy)phenyl]-3-(trifluoromethyl)benzamide | HCID 14405584 | — |
Reaction Steps
A solution of 12.5 g of 3.(trifluoromethyl)benzoyl chloride in 60 ml of dichloromethane is added dropwise to a suspension of 9.9 g of 2-(2-methylpropoxy)benzenamine and 33 g of potassium carbonate in 90 ml of dichloromethane, cooled in an ice-bath.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001159 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-10aee65a7c594b228059886e0d0602f6 |
| Source note | uspto-grants-1991_03 |