HRID359541

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID11430

Potassium Carbonate

CK2O3

HCID67561

alpha,alpha,alpha-Trifluoro-o-toluoyl chloride

C8H4ClF3O

HCID13654662

2-(2-Methylpropoxy)aniline

C10H15NO

PRODUCTS

生成物

结构：CC(C)COc1ccccc1NC(=O)c1cccc(C(F)(F)F)c1

HCID14405584

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6344

Dichloromethane

CH2Cl2

2 次

PROCEDURE

实验过程

A solution of 12.5 g of 3.(trifluoromethyl)benzoyl chloride in 60 ml of dichloromethane is added dropwise to a suspension of 9.9 g of 2-(2-methylpropoxy)benzenamine and 33 g of potassium carbonate in 90 ml of dichloromethane, cooled in an ice-bath.

WORKUP

后处理

temperaturecooled in an ice-bath