HuagongsheHuagongshe Chemistry Print Report · For research reference only
n-Octanoyl-5-salicylic acid → HCID 178442659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | n-Octanoyl-5-salicylic acid | HCID 9838158 | — |
| Reactant | Benzethonium carbonate | HCID 86744670 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178442659 | HCID 178442659 | 193.7% |
Reaction Steps
2.2 g (8.4 mmol) of 5-octanoylsalicylic acid, dissolved beforehand in 100 ml of methanol, are added to a solution of 3.7 g (4.2 mmol) of benzethonium carbonate dissolved in 100 ml of methanol; the mixture is stirred for 1 hour at room temperature, the solution is then filtered and the filtrate is evaporated to dryness to give 5.5 g (98% yield) of benzethonium 5-octanoylsalicylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001156 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-bf8c077ac18f44feba68d84a5a06ceef |
| Source note | uspto-grants-1991_03 |