HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Dodecanoylsalicylic acid → HCID 178442658, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Dodecanoylsalicylic acid | HCID 9797152 | — |
| Reactant | HCID 86744670 | HCID 86744670 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178442658 | HCID 178442658 | 192.1% |
Reaction Steps
2 g (6.4 mmol) of 5-dodecanoylsalicylic acid, dissolved beforehand in 100 ml of ethanol, are added to a solution of 2.82 g (3.2 mmol) of benzethonium carbonate dissolved in 100 ml of methanol; the mixture is stirred for 1 hour at room temperature, the solution is then filtered and the filtrate is evaporated to dryness to give 4.5 g (97% yield) of benzethonium 5-dodecanoylsalicylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001156 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-d3d404f71b0c453ba69cdfb61ad0b972 |
| Source note | uspto-grants-1991_03 |