HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → HCID 20063610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | HCID 23009735 | HCID 23009735 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20063610 | HCID 20063610 | — |
Reaction Steps
A mixture comprising 0.11 mole (26.6 g) of 2-amino-4-nitro-1,3,5-trimethoxybenzene and 55 ml of formic acid are refluxed during three hours. The reaction mixture is cooled and diluted with iced water. The expected product precipitates and is separated by filtration. After drying it is recrystallized from ethanol. It melts at 98° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05002585 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-29fa187fbf714e038a1767d6e11d47d9 |
| Source note | uspto-grants-1991_03 |