HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anisole → HCID 178503585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anisole | HCID 7519 | — |
| Reactant | Methyl triflate | HCID 9526 | — |
| Reactant | HCID 20064366 | HCID 20064366 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 178503585 | HCID 178503585 | — |
Reaction Steps
27 g of 6-methyl-2-methylcycloheptimidazole was added to 100 ml of anisole and stirred under cooling with ice. Next, 28 g of methyl trifluoromethanesulfonate was dropwise added and further everything was stirred under cooling with ice. After everything was stirred for 1 hour at room temperature, 200 ml of ethyl acetate was added, and the crystals precipitated were separated by filtration and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05003077 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-372a23129d09481db7728c198ba66752 |
| Source note | uspto-grants-1991_03 |