HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Chloride → HCID 15137712, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Chloride | HCID 4873 | — |
| Reactant | HCID 15137706 | HCID 15137706 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 15137712 | HCID 15137712 | 64.7% |
Reaction Steps
A mixture of 1.9 g of 1-[(4-butylphenyl)methyl]-1-[6-[(methylsulfonyl)oxy]hexyl]-3-(2,4,6-trichlorophenyl)urea, 0.6 g of potassium chloride, and 3.0 ml of dried dimethyl sulfoxide was heated at an oil bath temperature of 60°-70° C. for 20 hours. The extraction and chromatography procedures of Example 521 were followed to give 1.1 g of the desired product as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05003106 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-46709bbc712c497ab10aec2d5d213456 |
| Source note | uspto-grants-1991_03 |