Ammonium Hydroxide → 4-Butylbenzamide

HRID 359993ノート

反応式

HRID 359993 の反応式
[CH2:1]([C:5]1[CH:13]=[CH:12][C:8]([C:9](Cl)=[O:10])=[CH:7][CH:6]=1)[CH2:2][CH2:3][CH3:4].[OH-].[NH4+:15]>>[CH2:1]([C:5]1[CH:13]=[CH:12][C:8]([C:9]([NH2:15])=[O:10])=[CH:7][CH:6]=1)[CH2:2][CH2:3][CH3:4]

参加物

3

反応物 2

HCID 14923Ammonium HydroxideHCID 1200494-Butylbenzoyl chloride

生成物 1

HCID 28014584-Butylbenzamide収率 99%

実験手順

To a stirred solution of 200 ml of aqueous ammonium hydroxide was added dropwise 35 ml of 4-butylbenzoyl chloride. The resulting mixture was stirred at room temperature for several hours. The white solid was collected by filtration, washed with water, then hexane, and dried in vacuo at 60° C. to give 33.4 g (99% yield) of the desired product, mp 135°-136° C.

後処理

  1. filtrationThe white solid was collected by filtration
  2. washwashed with water
  3. dry with materialhexane, and dried in vacuo at 60° C.

出典と根拠

ORDレコード
ord-db0fba08642943098ae12ac99a4f0ced
出典データセット
uspto-grants-1991_03
特許番号
US05003106

反応ノート

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