HRID36020

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID70297

Benzenecarboperoxoic acid, 3-chloro-

C7H5ClO3

结构：CCCCc1nc(SC)c(C(=O)OCC)n1Cc1ccc(-c2ccccc2C(=O)OC)cc1

HCID21479063

未命名化合物

PRODUCTS

生成物

结构：CCCCc1nc(S(C)=O)c(C(=O)OCC)n1Cc1ccc(-c2ccccc2C(=O)O)cc1

HCID21479009

未命名化合物

收率 259.4%

PROCEDURE

实验过程

The operation is carried out as in Example 15 starting with 1.55 g of the product obtained in Example 21 using 213 mg of metachloroperbenzoic acid. 1.8 g of crude product is obtained which is chromatographed on silica (eluant: methylene chloride--acetone (7-3)). 1.5 g of desired product is obtained.

WORKUP

后处理

custom1.8 g of crude product is obtained which
customis chromatographed on silica (eluant: methylene chloride--acetone (7-3))