O-Xylene → HCID 18788042, compound

HRID 361287Notes

Reaction equation

HRID 361287 reaction equation
[CH2:1]([N:5](CC(C)=C)[C:6]1[CH:11]=CC=C[CH:7]=1)[CH2:2][CH2:3][CH3:4].[C:16]1([CH3:23])[C:17](C)=[CH:18][CH:19]=[CH:20][CH:21]=1>[Cl-].[Zn+2].[Cl-]>[CH2:1]([N:5]1[C:17]2[C:16](=[CH:21][CH:20]=[CH:19][CH:18]=2)[CH2:23][C:6]1([CH3:11])[CH3:7])[CH2:2][CH2:3][CH3:4]

Participants

4

Reactant 2

HCID 7237O-XyleneHCID 54010992N-butyl-N-(2-methylprop-2-eneyl)aniline

Product 1

HCID 18788042HCID 18788042, compound

Reagents, catalysts & solvents 1

HCID 3007855ZincchlorideCatalyst

Procedure

A mixture of N-butyl-N-(2-methylprop-2-eneyl)aniline (9.6 parts), zinc chloride (6.12 parts) and xylene (20 parts) was heated under reflux with vigorous stirring for 4.75 hours. The cooled mixture was filtered and the organic phase evaporated to leave 1-butyl-2,2-dimethylindoline (5.3 parts).

Workup

  1. temperaturewas heated
  2. temperatureunder reflux
  3. filtrationThe cooled mixture was filtered
  4. customthe organic phase evaporated

Sources & evidence

ORD record
ord-c307e14b853947698fc2fcb3cdb64320
Source dataset
uspto-grants-1999_02
Patent number
US05865857

Reaction notes

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