HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10664064, compound → HCID 10686415, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10664064 | HCID 10664064 | — |
| Reactant | HCID 10854804 | HCID 10854804 | — |
| Solvent | Acetone hexane | HCID 21880519 | — |
| Product | HCID 10686415 | HCID 10686415 | — |
Reaction Steps
Using a procedure similar to that described at Example 1 except replacing the 6β-propargyl-5α-hydroxyandrostane-3,17-dione (10) used therein with 6β-propargyl-5α-hydroxyestrane-3,17-dione (11), the title compound was prepared; 60%; m.p. 194°-195° C. (from acetone/hexane); 1H-NMR (CDCl3) δ 0.94 (s, 3H, 18-CH3), 2.73 (m, 1H), 5.94 (s, 1H, 4-H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05866558 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-f965206eb15349feb8a0fc926d459296 |
| Source note | uspto-grants-1999_02 |