HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 86753644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 178426683 | HCID 178426683 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86753644 | HCID 86753644 | — |
Reaction Steps
To a stirred solution of 620 mg (0.29 mmol) of 2-t-butyloxycarbonylamino-3-methylpyridine-N-oxide in 8 mL of CH2Cl2 under Ar was added 262 μL (0.3 mmol) of dimethyl sulfate. The CH2Cl2 was allowed to evaporate under a slow stream of Ar overnight to give the title compound as a light tan solid:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05866573 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-ae23a3f837344aa7bf5b2683f5033469 |
| Source note | uspto-grants-1999_02 |