HRID361566

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：O=C1[C@H]2CCC[C@H]2Nc2ccccc2N1Cc1cccc([N+](=O)[O-])c1

HCID54235912

未命名化合物

PRODUCTS

生成物

结构：Nc1cccc(CN2C(=O)[C@H]3CCC[C@H]3Nc3ccccc32)c1

HCID54512889

未命名化合物

收率 84%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

Using (3aR*,10aS*)-9-(3-nitrobenzyl)-2,3,3a,4,9,10a-hexahydrobenzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one, the title compound was synthesized in otherwise the same manner as Reference Example 7. Yield 84%, m.p. 176°-178° C. (diethyl ether).