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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 361586Generated: October 30, 2026

Diethyl ether ethanol → HCID 54563692, compound

https://huagongshe.com/reaction/361586

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl ether ethanolHCID 21585056—
ReactantHCID 86753653HCID 86753653—
ProductHCID 54563692HCID 5456369235%

Reaction Steps

Using (3aR*,10aS*)-4-(chloroacetyl)-9-[4-[3-(4-fluorobenzyl)ureido]benzyl]-2,3,3a,4,9,10a-hexahydrobenzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one, the title compound was synthesized in otherwise the same manner as Example 30. Yield 35%, m.p. 154°-156° C. (ethanol-diethyl ether).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05866567
Source datasetuspto-grants-1999_02
ORD IDord-5f30dd94ee854e9c8192f4e5ee0619b3
Source noteuspto-grants-1999_02