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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 361587Generated: October 30, 2026

Diethyl ether ethanol → HCID 53729474, compound

https://huagongshe.com/reaction/361587

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethyl ether ethanolHCID 21585056—
ReactantHCID 54005651HCID 54005651—
ProductHCID 53729474HCID 5372947438%

Reaction Steps

Using (3aR*,10aS*)-4-(chloroacetyl)-9-[4-[3-(4-methoxybenzyl)ureido]benzyl]-2,3,3a,4,9,10a-hexahydro-benzo[b]cyclopenta[e][1,4]diazepin-10(1H)-one, the title compound was synthesized in otherwise the same manner as Example 30. Yield 38%, m.p. 155.5°-158.5° C. (ethanol-diethyl ether).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05866567
Source datasetuspto-grants-1999_02
ORD IDord-c000a1a08a09455280b7b1afaa299e7f
Source noteuspto-grants-1999_02