HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenethylamine → HCID 2450326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenethylamine | HCID 1001 | — |
| Reactant | Ethyl 2-pyridinecarboxylate | HCID 17307 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 2450326 | HCID 2450326 | — |
Reaction Steps
A mixture of 20 ml of ethyl pyridine-2-carboxylate and 27 ml of phenethylamine was stirred at 180° C. for 5 h., with the ethanol formed being distilled off over a 30 cm Vigreux column. Distillation of the residue yielded 30.9 g of pyridine-2-carboxylic acid phenethyl-amide as a yellowish oil, b.p. 150°-155° C./0.8 mbar.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05866583 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-ebdf5ff3e2cc450aac0103a139a62c9f |
| Source note | uspto-grants-1999_02 |