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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 361716Erstellt: 25. Oktober 2026

Water → Propionitrile, 3-(p-chlorophenoxy)-

https://huagongshe.com/reaction/361716

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktWaterHCID 962—
Edukt4-ChlorophenolHCID 4684—
EduktAcrylonitrileHCID 7855—
EduktBenzyltrimethylammonium hydroxideHCID 66854—
LösungsmittelMethanolHCID 887—
ProduktPropionitrile, 3-(p-chlorophenoxy)-HCID 96550—

Reaktionsschritte

A mixture of p-chlorophenol (25 g), acrylonitrile (30 ml) and a solution of benzyltrimethylammonium hydroxide (8 ml of a 40 wt % solution in methanol) were heated at reflux over the weekend. The reaction mixture was poured into water and extracted with ethyl acetate. The ethyl acetate extract was dried and evaporated to give 3-(4-chlorophenoxy)propionitrile.

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS05866611
Quelldatensatzuspto-grants-1999_02
ORD IDord-525446a4cf4c4e54862c339880ef50f7
Quellennotizuspto-grants-1999_02