HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Water → Propionitrile, 3-(p-chlorophenoxy)-
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Water | HCID 962 | — |
| Edukt | 4-Chlorophenol | HCID 4684 | — |
| Edukt | Acrylonitrile | HCID 7855 | — |
| Edukt | Benzyltrimethylammonium hydroxide | HCID 66854 | — |
| Lösungsmittel | Methanol | HCID 887 | — |
| Produkt | Propionitrile, 3-(p-chlorophenoxy)- | HCID 96550 | — |
Reaktionsschritte
A mixture of p-chlorophenol (25 g), acrylonitrile (30 ml) and a solution of benzyltrimethylammonium hydroxide (8 ml of a 40 wt % solution in methanol) were heated at reflux over the weekend. The reaction mixture was poured into water and extracted with ethyl acetate. The ethyl acetate extract was dried and evaporated to give 3-(4-chlorophenoxy)propionitrile.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05866611 |
| Quelldatensatz | uspto-grants-1999_02 |
| ORD ID | ord-525446a4cf4c4e54862c339880ef50f7 |
| Quellennotiz | uspto-grants-1999_02 |