反应详情

A mixture of p-chlorophenol (25 g), acrylonitrile (30 ml) and a solution of benzyltrimethylammonium hydroxide (8 ml of a 40 wt % solution in methanol) were heated at reflux over the weekend. The reaction mixture was poured into water and extracted with ethyl acetate. The ethyl acetate extract was dried and evaporated to give 3-(4-chlorophenoxy)propionitrile.

1. temperatureat reflux over the weekend
2. extractionextracted with ethyl acetate
3. extractionThe ethyl acetate extract
4. customwas dried
5. customevaporated