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HRID362055

反应详情

EQUATION

反应方程式

HRID 362055 的结构方程式

REACTANTS

反应物

2
结构：CC1(C)CNCCN1
HCID14664186

2,2-Dimethylpiperazine

C6H14N2

结构：COc1ccc(CS[C@H]2C[C@@H](C(=O)O)N(C(=O)OCc3ccc([N+](=O)[O-])cc3)C2)cc1
HCID15297071

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)CN(C(=O)[C@@H]2C[C@H](S)CN2C(=O)OCc2ccc([N+](=O)[O-])cc2)CCN1C(=O)OCc1ccc([N+](=O)[O-])cc1
HCID88319373

未命名化合物

收率 106%

PROCEDURE

实验过程

Following a procedure similar to that described in Preparation 38, but using 0.35 g of (2S,4S)-4-(4-methoxybenzylthio)-1-(4-nitrobenzyloxycarbonyl)-2-pyrrolidinecarboxylic acid, 0.15 g of N,N'-carbonyldiimidazole and 0.13 g of 2,2-dimethylpiperazine, 250 mg of the title compound were obtained as an amorphous solid.

WORKUP

后处理

  1. customthat described in Preparation 38