Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 362537Generated: October 31, 2026

HCID 15434320, compound → HCID 21224732, compound

https://huagongshe.com/reaction/362537

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15434320HCID 15434320—
ReactantTrifluoroacetic acid methylene chlorideHCID 21863450—
ProductHCID 21224732HCID 21224732—

Reaction Steps

The resin 15 (0.075 mmol) is treated with 10%, TFA/CH2Cl2 (2.5 mL) at room temperature for 4.5 hours and filtered. The resin is rinsed with CH2Cl2 (2×3 mL), MeOH (2×3 mL), and the combined filtrates are evaporated and dried to afford 16.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05869579
Source datasetuspto-grants-1999_02
ORD IDord-d4ed61f2b3184ab5a81f5c8b174ca05d
Source noteuspto-grants-1999_02