HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19353659, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Reactant | 3-Methylisothiazol-5-ylamine hydrochloride | HCID 2723918 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19353659 | HCID 19353659 | — |
Reaction Steps
From methoxyacetyl chloride and 3-methyl-isothiazol-5-ylamine hydrochloride with triethylamine in dichloromethane. Then treatment with a borane-dimethyl sulphide complex in tetrahydrofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05869500 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-f68fe66a57224eed8d128dfd1bd906b5 |
| Source note | uspto-grants-1999_02 |