HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 15346385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | HCID 53746681 | HCID 53746681 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 15346385 | HCID 15346385 | — |
Reaction Steps
5.0 g (19.7 mmol) 5-Amino-1-(5-difluoromethoxy-1-methyl-3-pyrazolyl)-4-pyrazolecarbonitrile was dissolved in 180 ml acetonitrile and 2.65 g (19.7 mmol) sulfuryl chloride added dropwise. The mixture was stirred for one hour at room temperature and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05869686 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-ab1aa04b68bc471cb27c3c641dc7393a |
| Source note | uspto-grants-1999_02 |