HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 54055627, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 54153912 | HCID 54153912 | — |
| Solvent | 1,2-Dichloroethane | HCID 11 | — |
| Product | HCID 54055627 | HCID 54055627 | — |
Reaction Steps
0.2 g (3.8 mmol) 1-(5-Difluoromethoxy-1-methyl-3-pyrazolyl)-5-methyl-4-pyrazolecarboxylic acid was suspended in 30 ml 1,2-dichloroethane and 1.19 g (10.0 mmol) thionyl chloride was added at room temperature, dropwise. The mixture was heated for 1 hour under reflux and concentrated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05869686 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-c5fded5ebf694bcaaae84dee4e16dfe4 |
| Source note | uspto-grants-1999_02 |