Hydrochloric Acid → HCID 178499561, compound

HRID 362701Notes

Reaction equation

HRID 362701 reaction equation
[ClH:1].[NH:2]1[CH:6]=[C:5]([CH2:7][C:8]([OH:10])=[O:9])[N:4]=[CH:3]1.Cl.[CH3:12]O>>[ClH:1].[CH3:12][O:9][C:8](=[O:10])[CH2:7][C:5]1[N:4]=[CH:3][NH:2][CH:6]=1

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 178479752HCID 178479752, compound

Product 1

HCID 178499561HCID 178499561, compound

Procedure

A solution of 1H-imidazole-4-acetic acid hydrochloride (4.00 g, 24.6 mmol) in methanol (100 ml) was saturated with gaseous hydrogen chloride. The resulting solution was allowed to stand at room temperature (RT) for 18 hours. The solvent was evaporated in vacuo to afford the title compound as a white solid.

Workup

  1. customto stand at room temperature
  2. custom(RT)
  3. customfor 18 hours
  4. customThe solvent was evaporated in vacuo

Sources & evidence

ORD record
ord-1e5c33fe53a6457a98e7ff0d4d2a6881
Source dataset
uspto-grants-1999_02
Patent number
US05869682

Reaction notes

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