HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 23293624, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 23293654 | HCID 23293654 | — |
| Catalyst | Dichloromethane | HCID 6344 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 23293624 | HCID 23293624 | — |
Reaction Steps
A suspension of (E)-2-(4-chloro-1-indanylidene)acetic acid (5.5 g, 0.03 mol) in a mixture of dimethylformamide: dichloromethane (5 drops: 50 mL) was treated with oxalyl chloride (6.6 g, 0.05 mol) and allowed to stir at room temperature for 18 h. The resulting solution was concentrated in vacuo and the residue used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05872118 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-1c7d343ef5e4487499a9e65b5b77fbdc |
| Source note | uspto-grants-1999_02 |