Ethylparaben → Ethyl 4-(2-cyclohexylethoxy)benzoate

HRID 363026Notes

Reaction equation

[CH:1]1([CH2:7][CH2:8][OH:9])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.O[C:11]1[CH:21]=[CH:20][C:14]([C:15]([O:17][CH2:18][CH3:19])=[O:16])=[CH:13][CH:12]=1>>[CH:1]1([CH2:7][CH2:8][O:9][C:11]2[CH:21]=[CH:20][C:14]([C:15]([O:17][CH2:18][CH3:19])=[O:16])=[CH:13][CH:12]=2)[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1

Participants

Reactant 2

HCID 8434Ethylparaben

HCID 205082-Cyclohexylethanol

Product 1

HCID 54484113Ethyl 4-(2-cyclohexylethoxy)benzoate

Procedure

2-Cyclohexylethanol 15-1 (3.2 g, 25 mmol) and ethyl 4-hydroxybenzoate 15-2 (4.15 g, 25 mmol) were reacted as in Example 14. The product 15-3 was obtained as a waxy solid.

Sources & evidence

ORD record: ord-8276584a95414161b4aadb7390820eea
Source dataset: uspto-grants-1999_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05872138

Reaction notes

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