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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 36311Generated: October 30, 2026

Thionyl Chloride → 5-Hexylthiophene-2-carboxylic acid chloride

https://huagongshe.com/reaction/36311

Reaction equation

Participants

RoleNameHCIDCharge
ReactantThionyl ChlorideHCID 24386—
Reactant5-Hexylthiophene-2-carboxylateHCID 19938024—
Product5-Hexylthiophene-2-carboxylic acid chlorideHCID 13128272—

Reaction Conditions

Temperature80 °C

Reaction Steps

10 m of thionyl chloride was added to 1.0 g (4.72×10-3 mol) of 5-hexylthiophene-2-carboxylate and the mixture was stirred for 4 hours at 80° C., followed by removal of excess thionyl chloride, whereby 5-hexylthiophene-2-carboxylic acid chloride was obtained.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05413735
Source datasetuspto-grants-1995_05
ORD IDord-c896d179ae094facb36b1fd49d84e5cd
Source noteuspto-grants-1995_05