化工社化工社 化学情報印刷レポート · 研究参考用
Water → 5-phenylpyridine-2-carboxylic Acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | 2-Methyl-5-phenylpyridine | HCID 76744 | — |
| 反応物 | Potassium Permanganate | HCID 516875 | — |
| 生成物 | 5-phenylpyridine-2-carboxylic Acid | HCID 2762870 | — |
反応手順
A suspension of 3-phenyl-6-methyl pyridine (1.99 g, 11.78 mmol) and potassium permanganate (7.65, 48.6 mmol), in water (50 mL) was heated at reflux for 16 hours. The reaction was allowed to cool to ambient temperature and filtered through celite to remove the solids. Acetic acid (2 mL) was added to the colourless filtrate and the product was collected as a white solid by filtration.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05872136 |
| 出典データセット | uspto-grants-1999_02 |
| ORD ID | ord-343691b2d04c48aca1c08a10cca1ee35 |
| 出典メモ | uspto-grants-1999_02 |