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HRID 363187作成日:2026年10月25日

Water → 5-phenylpyridine-2-carboxylic Acid

https://huagongshe.com/reaction/363187

反応式

関与物質

役割名称HCID仕込み量
反応物WaterHCID 962—
反応物2-Methyl-5-phenylpyridineHCID 76744—
反応物Potassium PermanganateHCID 516875—
生成物5-phenylpyridine-2-carboxylic AcidHCID 2762870—

反応手順

A suspension of 3-phenyl-6-methyl pyridine (1.99 g, 11.78 mmol) and potassium permanganate (7.65, 48.6 mmol), in water (50 mL) was heated at reflux for 16 hours. The reaction was allowed to cool to ambient temperature and filtered through celite to remove the solids. Acetic acid (2 mL) was added to the colourless filtrate and the product was collected as a white solid by filtration.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05872136
出典データセットuspto-grants-1999_02
ORD IDord-343691b2d04c48aca1c08a10cca1ee35
出典メモuspto-grants-1999_02