HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Ethylhexyloxy)ethanol → HCID 4089548, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Ethylhexyloxy)ethanol | HCID 15260 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | HCID 4089548 | HCID 4089548 | 94.2% |
Reaction Steps
500 g (2.81 mol) of 2-(2-ethylhexyloxy)ethanol and 500 g of thionyl chloride were placed in a 2-liter four-neck flask and refluxed with heat for 2 hours. Subsequently, a distillation under reduced pressure was conducted to obtain 510 g of 2-(2-ethylhexyloxy)ethylchloride as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05872272 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-36df7e95c51846788f77bd32bd1c86af |
| Source note | uspto-grants-1999_02 |