HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,8-Diazabicyclo(5.4.0)undec-7-ene → N-(4-vinylbenzoyl)methanesulfonarnide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,8-Diazabicyclo(5.4.0)undec-7-ene | HCID 81184 | — |
| Reactant | N-[4-(2-bromoethyl)benzoyl]methanesulfonamide | HCID 67587437 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-(4-vinylbenzoyl)methanesulfonarnide | HCID 15404408 | — |
Reaction Steps
N-(4-vinylbenzoyl)methanesulfonarnide was prepared according to step 2 of Example 1 from N-[4-(2-bromoethyl)benzoyl]methanesulfonamide and 1,8-diazabicyclo-[5.4.0]undec-7-ene (DBU) in THF.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05874194 |
| Source dataset | uspto-grants-1999_02 |
| ORD ID | ord-a357ccf380414d7d9bb3faa812baec81 |
| Source note | uspto-grants-1999_02 |