1,8-Diazabicyclo(5.4.0)undec-7-ene → N-(4-vinylbenzoyl)methanesulfonarnide

HRID 363283Notes

Reaction equation

HRID 363283 reaction equation
Br[CH2:2][CH2:3][C:4]1[CH:16]=[CH:15][C:7]([C:8]([NH:10][S:11]([CH3:14])(=[O:13])=[O:12])=[O:9])=[CH:6][CH:5]=1.N12CCCN=C1CCCCC2>C1COCC1>[CH:3]([C:4]1[CH:16]=[CH:15][C:7]([C:8]([NH:10][S:11]([CH3:14])(=[O:12])=[O:13])=[O:9])=[CH:6][CH:5]=1)=[CH2:2]

Participants

4

Reactant 2

HCID 811841,8-Diazabicyclo(5.4.0)undec-7-eneHCID 67587437N-[4-(2-bromoethyl)benzoyl]methanesulfonamide

Product 1

HCID 15404408N-(4-vinylbenzoyl)methanesulfonarnide

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

N-(4-vinylbenzoyl)methanesulfonarnide was prepared according to step 2 of Example 1 from N-[4-(2-bromoethyl)benzoyl]methanesulfonamide and 1,8-diazabicyclo-[5.4.0]undec-7-ene (DBU) in THF.

Sources & evidence

ORD record
ord-a357ccf380414d7d9bb3faa812baec81
Source dataset
uspto-grants-1999_02
Patent number
US05874194

Reaction notes

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